Triethylamine → N,N'-bis(allyl)carbodiimide
Reaction equation
[CH2:1]([NH:4][C:5]([NH:7][CH2:8][CH:9]=[CH2:10])=S)[CH:2]=[CH2:3].C(N(CC)CC)C.[I-].ClC1C=CC=C[N+]=1C>C(#N)C>[CH2:1]([N:4]=[C:5]=[N:7][CH2:8][CH:9]=[CH2:10])[CH:2]=[CH2:3]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
1.56 g of N,N'-bis(allyl)thiourea, 2.4 g of triethylamine and 3.07 g of 2-chloro-1-methylpyridinium iodide are reacted in 40 ml of acetonitrile and the reaction mixture is worked up as described in Example 4. The product is obtained as a faintly yellowish oil.
Workup
- customThe product is obtained as a faintly yellowish oil
Sources & evidence
- ORD record
- ord-b1e719b11ff545e7ba7de4d2f9e2dd6e
- Source dataset
- uspto-grants-1989_08
- Patent number
- US04859761
Reaction notes
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