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Hydrochloric Acid → HCID 86023621, compound

HRID 1724715
Notes
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Reaction equation

HRID 1724715 reaction equation
Cl.[C:2]([CH:4]([P:12](=[O:19])([O:16][CH2:17][CH3:18])[O:13][CH2:14][CH3:15])[CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)#[N:3]>CCO.[Pt]=O>[NH2:3][CH2:2][CH:4]([P:12](=[O:19])([O:13][CH2:14][CH3:15])[O:16][CH2:17][CH3:18])[CH2:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1
ParticipantsProcedureSources & evidenceReaction notes

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 281202Diethyl(1-cyano-2-phenylethyl)phosphonate

Product 1

HCID 86023621HCID 86023621, compound

Reagents, catalysts & solvents 2

HCID 82844Platinum oxide (PtO)CatalystHCID 702EthanolSolvent

Procedure

Platinum oxide and conc.HCl were added to a solution of diethyl (1-cyano-2-phenylethyl)phosphonate in EtOH, for overnight stirring under hydrogen atmosphere, to obtain diethyl [2-amino-1-(cyclohexylmethyl)ethyl]phosphonate.

Sources & evidence

ORD record
ord-0c896b0f54b14705b1b8c73832637720
Source dataset
uspto-grants-2009_02
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07488739B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes