3-(Tetradecyloxy)benzoic acid → 3-(Tetradecyloxy)benzenemethanol

HRID 1728809

Reaction equation

HRID 1728809 reaction equation
[CH2:1]([O:15][C:16]1[CH:17]=[C:18]([CH:22]=[CH:23][CH:24]=1)[C:19](O)=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH2:1]([O:15][C:16]1[CH:17]=[C:18]([CH2:19][OH:20])[CH:22]=[CH:23][CH:24]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 2

HCID 32623113-(Tetradecyloxy)benzoic acidHCID 21226445Aluminium lithium hydride

Product 1

HCID 100417103-(Tetradecyloxy)benzenemethanol

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The title compound is prepared by the procedure of Example 21 using 20.0 g of product from Example 23, 200 ml of dry tetrahydrofuran and 7.94 g of lithium aluminum hydride. The product, 18.82 g, is obtained as colorless crystals.

Workup

  1. customThe product, 18.82 g, is obtained as colorless crystals

Sources & evidence

ORD record
ord-141953c22b7945be92b2989240ca8b93
Source dataset
uspto-grants-1994_07
Patent number
US05328921

Linked notes

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