Vinyl stearate → Vinyloxycarbonylmethyl salicylate vinyl stearate

HRID 1730259Notes

Reaction equation

HRID 1730259 reaction equation
[Pb].[N].[C:3]([O-:12])(=[O:11])[C:4]1[C:5](=[CH:7][CH:8]=[CH:9][CH:10]=1)[OH:6].[Na+].C(C(Cl)C([O-])=O)=C.[C:21]([O:40][CH:41]=[CH2:42])(=[O:39])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH3:38]>CN(C)C=O>[C:3]([O:12][CH2:22][C:21]([O:40][CH:41]=[CH2:42])=[O:39])(=[O:11])[C:4]1[C:5](=[CH:7][CH:8]=[CH:9][CH:10]=1)[OH:6].[C:21]([O:40][CH:41]=[CH2:42])(=[O:39])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH3:38]

Participants

6

Reactant 4

HCID 66077Vinyl stearateHCID 16760658Sodium SalicylateHCID 20393230VinylchloroacetateHCID 178514658HCID 178514658, compound

Product 1

HCID 20314143Vinyloxycarbonylmethyl salicylate vinyl stearate

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are introduced 1.6 g of sodium salicylate, 4 g of a copolymer composed of 30% vinylchloroacetate and 70% of vinyl stearate (MW = 40,000) and 20 g of dimethylformamide.

Workup

  1. customInto a 50 ml flask provided with a condenser

Sources & evidence

ORD record
ord-c379b9d5e3a14676bd19ed870144e3db
Source dataset
uspto-grants-1976_11
Patent number
US03992356

Reaction notes

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