Hydrazine hydrate (1:1) → 2-(C-phenylcarbonohydrazonoyl)aniline

HRID 1730453Notes

Reaction equation

HRID 1730453 reaction equation
[NH2:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=O.O.[NH2:17][NH2:18]>C(O)COCCO>[NH2:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[C:4](=[N:17][NH2:18])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 760802-Aminobenzophenone

Product 1

HCID 6111762-(C-phenylcarbonohydrazonoyl)aniline

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In the manner given in Preparation 1, 2-aminobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-aminobenzophenone hydrazone.

Sources & evidence

ORD record
ord-6473e672e1ad441987fe6541e68a2edd
Source dataset
uspto-grants-1976_11
Patent number
US03992400

Reaction notes

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