Propanenitrile, 3-ethoxy- → HCID 20228183, compound

HRID 1731653

Reaction equation

HRID 1731653 reaction equation
[Na].[Cl:2][C:3]1[CH:4]=[CH:5][C:6]([NH:9][NH2:10])=[N:7][CH:8]=1.C(O[CH2:14][CH2:15][C:16]#[N:17])C>C(O)C>[NH2:17][C:16]1[CH2:15][CH2:14][N:9]([C:6]2[CH:5]=[CH:4][C:3]([Cl:2])=[CH:8][N:7]=2)[N:10]=1

Participants

5

Reactant 3

HCID 16501Propanenitrile, 3-ethoxy-HCID 5360545SodiumHCID 135904645-Chloro-2-hydrazinylpyridine

Product 1

HCID 20228183HCID 20228183, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 0.08 g. amount of sodium metal is dissolved in 10 ml. of absolute ethanol, then 2.5 g. of 5-chloro-2-hydrazinopyridine is added, followed by 1.70 g. of beta-ethoxypropionitrile. The procedure of Example 1 is continued to give 1.40 g. of the product of the Example as yellow crystals, m.p. 203°-204.5° C.

Workup

  1. customto give 1.40 g

Sources & evidence

ORD record
ord-0dd7695bf24943a1b0dc259beb62d8ac
Source dataset
uspto-grants-1986_11
Patent number
US04622401

Linked notes

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