Hydroxylamine → HCID 86704403, compound

Reaction equation

[CH2:1]1[C:3]2([CH2:8][CH2:7][CH2:6][CH2:5][CH:4]2[CH:9]=O)[CH2:2]1.[NH2:11][OH:12]>>[CH2:1]1[C:3]2([CH2:8][CH2:7][CH2:6][CH2:5][CH:4]2[CH:9]=[N:11][OH:12])[CH2:2]1

Participants

Reactant 2

HCID 787Hydroxylamine

HCID 59001176Spiro[2.5]octane-4-carbaldehyde

Product 1

HCID 86704403HCID 86704403, compound

Procedure

Spiro[2.5]octane-4-carbaldehyde oxime (I-11I) was prepared by reaction of spiro[2.5]octane-4-carbaldehyde and hydroxylamine following the same procol as described for I-6c. MS m/z 154.1 (M+1).

Sources & evidence

ORD record: ord-5783e702d4ca41b6a82573a759bcab91
Source dataset: uspto-grants-2015_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09150568B2

Reaction notes

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