Hydrochloric Acid → HCID 85866484, compound

HRID 1763188

Reaction equation

HRID 1763188 reaction equation
[CH3:1][N:2]1[CH2:7]N(C)CN(C)C1.[C:10]([S:18]CN)([CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:12])[CH3:11].[ClH:21]>C(#N)C>[ClH:21].[CH3:1][NH:2][CH2:7][S:18][C:10]([CH2:13][C:14]([CH3:17])([CH3:16])[CH3:15])([CH3:12])[CH3:11]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 79521,3,5-Trimethyl-1,3,5-triazacyclohexaneHCID 86735983HCID 86735983, compound

Product 1

HCID 85866484HCID 85866484, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

300 ml. of acetonitrile, 12.9 g. (0.1 mole) of 1,3,5-trimethylhexahydro-s-triazine; 43.8 g. (0.3 mole) of tert.-octylthiomethylamine and 12 g. of hydrogen chloride gas are reacted together in the manner of Example I. A yield of 43.7 g. (64.6% of theory) of the title compound is obtained.

Sources & evidence

ORD record
ord-dba2278fae3647809136087c4a36efe9
Source dataset
uspto-grants-1978_09
Patent number
US04111682

Linked notes

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