Methylamine → HCID 178484937, compound
Reaction equation
[C:1]([NH:3][C:4](=[N:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][OH:17])=[CH:11][CH:10]=1)SC)#[N:2].[CH3:18][NH2:19]>CO>[C:1]([NH:3][C:4]([NH:19][CH3:18])=[N:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][OH:17])=[CH:11][CH:10]=1)#[N:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 0.42 g (0.00168 mol) of N-cyano-N'-[4-(2-hydroxyethyl)benzyl]-S-methylisothiourea in 50 ml of methanol and 10 g of methylamine was stirred at room temperature overnight. Evaporation of the solvent gave the title compound.
Workup
- customEvaporation of the solvent
Sources & evidence
- ORD record
- ord-9c1c7be5dc37482b9254a181f9161fc1
- Source dataset
- uspto-grants-1997_05
- Patent number
- US05633247
Reaction notes
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