Hydrazine hydrate (1:1) → HCID 59293631, compound
Reaction equation
Cl[C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([F:19])=[CH:15][CH:14]=2)[N:3]=1.O.[NH2:21][NH2:22]>>[F:19][C:16]1[CH:17]=[CH:18][C:13]([NH:12][C:4]2[N:3]=[C:2]([NH:21][NH2:22])[N:10]=[C:9]3[C:5]=2[N:6]=[CH:7][N:8]3[CH3:11])=[CH:14][CH:15]=1Participants
3
Procedure
Was prepared according to Example 8 from (2-chloro-9-methyl-9H-purin-6-yl)-(4-fluoro-phenyl)-amine and hydrazine monohydrate.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-4d018709e7da47949b5b3cdb14a5db3c
- Source dataset
- uspto-grants-2013_01
- Patent number
- US08362024B2
Reaction notes
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