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Pinacol → 2-(3-Bromophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1822668
Notes
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Reaction equation

HRID 1822668 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([B:8]([OH:10])[OH:9])[CH:5]=[CH:6][CH:7]=1.O[C:12]([C:15](O)([CH3:17])[CH3:16])([CH3:14])[CH3:13]>>[Br:1][C:2]1[CH:3]=[C:4]([B:8]2[O:10][C:15]([CH3:17])([CH3:16])[C:12]([CH3:14])([CH3:13])[O:9]2)[CH:5]=[CH:6][CH:7]=1
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 6425PinacolHCID 2734318(3-Bromophenyl)boronic acid

Product 1

HCID 99939532-(3-Bromophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneYield 77%

Procedure

The title compound (77%, oil) was prepared from 3-bromophenylboronic acid and pinacol.

Sources & evidence

ORD record
ord-6eead45df83e46a7984eb63ceab382ab
Source dataset
uspto-grants-2006_05
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07037905B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes