Hydrochloric Acid → HCID 18950271, compound
Reaction equation
Cl[C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=O)=[C:4]([Cl:11])[C:3]=1C.[CH:13]([O-:18])([O-])[O:14][CH2:15][CH3:16].[ClH:19]>C(O)C>[Cl:11][C:4]1[C:5]([CH3:6])=[C:9]([CH:10]=[CH:2][C:3]=1[Cl:19])[C:13]([O:14][CH2:15][CH3:16])=[O:18]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
12.0 g. (0.058 mol.) of dichloro-3-methylbenzoic acid and 75 ml. of ethyl orthoformate in 100 ml. of ethanol was saturated with hydrogen chloride and refluxed to give ethyl 3,4-dichloro-2-methylbenzoate.
Workup
- temperaturerefluxed
Sources & evidence
- ORD record
- ord-6f3afbae7dbc4c8187f65b1d12814a89
- Source dataset
- uspto-grants-1980_08
- Patent number
- US04218464
Reaction notes
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