2,3-Dinitrophenol → 1-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene

HRID 18599

Reaction equation

HRID 18599 reaction equation
[N+:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[CH:8][CH:7]=[CH:6][C:5]=1[OH:13])([O-:3])=[O:2].Cl[CH2:15][CH2:16][O:17][CH2:18][CH3:19]>>[CH2:16]([O:17][CH2:18][CH2:19][O:13][C:5]1[CH:6]=[CH:7][CH:8]=[C:9]([N+:10]([O-:12])=[O:11])[C:4]=1[N+:1]([O-:3])=[O:2])[CH3:15]

Participants

3

Reactant 2

HCID 61912,3-DinitrophenolHCID 12341Ethane, 1-chloro-2-ethoxy-

Product 1

HCID 867611331-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene

Procedure

1-(2-Ethoxy-ethoxy)-2,3-dinitro-benzene was prepared by a procedure according to example 108 (i) starting from 500 mg (2.72 mmol) 2,3-dinitro-phenol and 0.72 mL (6.52 mmol) 1-chloro-2-ethoxy-ethane. Yield: 450 mg MS (ES+): m/e=257.

Sources & evidence

ORD record
ord-c6240d9049d04e7597bd4c2718148baa
Source dataset
uspto-grants-2010_06
Patent number
US07741341B2

Linked notes

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