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5-Chlorosalicylic Acid → 5-chloro-N-(3,5-dichlorophenyl)-2-hydroxybenzamide

HRID 1865377
Notes
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Reaction equation

HRID 1865377 reaction equation
[Cl:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[Cl:12][C:13]1[CH:14]=[C:15]([CH:17]=[C:18]([Cl:20])[CH:19]=1)[NH2:16]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:11])=[C:6]([CH:10]=1)[C:7]([NH:16][C:15]1[CH:14]=[C:13]([Cl:12])[CH:19]=[C:18]([Cl:20])[CH:17]=1)=[O:9]
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 94475-Chlorosalicylic AcidHCID 122813,5-Dichloroaniline

Product 1

HCID 28046665-chloro-N-(3,5-dichlorophenyl)-2-hydroxybenzamideYield 41.2%

Procedure

Using 5-chlorosalicylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the Example 1(1) gave the title compound.

Sources & evidence

ORD record
ord-75a57ff4941a4167a757193b97174048
Source dataset
uspto-grants-2009_12
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07626042B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes