Silver Nitrate → Acesulfame silver

HRID 1883215

Reaction equation

HRID 1883215 reaction equation
[N+]([O-])([O-])=O.[Ag+:5].[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[N-:11][C:9](=[O:10])[CH:8]=1.[K+]>O>[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[NH:11][C:9](=[O:10])[CH:8]=1.[Ag:5]

Participants

4

Reactant 2

HCID 24470Silver NitrateHCID 11074431Acesulfame Potassium

Product 1

HCID 131724477Acesulfame silverYield 88%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of 30 mmol (5.148 g) of silver(I) nitrate in 30 ml of water was added to a solution of 30 mmol (6.037 g) of acesulfame-K in 30 ml of water. After addition was complete, the colorless precipitate formed was filtered off by suction and washed twice, each time with 10 ml of water. 88% of colorless acesulfame-silver crystals resulted. The reaction and subsequent workup as described above need not be carried out in the absence of light.

Workup

  1. additionAfter addition
  2. customthe colorless precipitate formed
  3. filtrationwas filtered off by suction
  4. washwashed twice

Sources & evidence

ORD record
ord-a719c7edd0914d6fa57be7d45727584e
Source dataset
uspto-grants-2004_07
Patent number
US06759544B2

Linked notes

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