Triethylsilane → HCID 69000417, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:13][C:12]([CH:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)O)=[CH:11][CH:10]=2)=[CH:5][CH:4]=1.C([SiH](CC)CC)C>>[CH2:14]([C:12]1[S:13][C:9]([C:6]2[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=2)=[CH:10][CH:11]=1)[C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1

Participants

Reactant 2

HCID 12052Triethylsilane

HCID 68998767HCID 68998767, compound

Product 1

HCID 69000417HCID 69000417, compoundYield 99%

Procedure

The title compound was prepared from the product of step 2 (0.6 g, 2.0 mmol) and triethylsilane (2.4 g, 20.2 mmol) using the procedure of Example 159, step 3 with 99% yield (0.55 g).

Sources & evidence

ORD record: ord-b4a19e90e0e849de87ffac856379952a
Source dataset: uspto-grants-2013_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08598359B2

Reaction notes

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