Phenyl Isothiocyanate → HCID 178496202, compound

Reaction equation

[NH:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][O:10][CH2:11][CH2:12][O:13][CH3:14])=[CH:5][N:4]=1)[NH2:2].N(C1C=CC=CC=1)=[C:16]=[S:17].BrC1C=CC2N(C(S)=NN=2)C=1>>[CH3:14][O:13][CH2:12][CH2:11][O:10][CH2:9][C:6]1[CH:7]=[CH:8][C:3]2[N:4]([C:16]([SH:17])=[N:2][N:1]=2)[CH:5]=1

Participants

Reactant 3

HCID 7673Phenyl Isothiocyanate

HCID 592331002-Hydrazinyl-5-((2-methoxyethoxy)methyl)pyridine

HCID 1785279206-Bromo-[1,2,4]triazolo[4,3-a]pyridine-3-thiol

Product 1

HCID 178496202HCID 178496202, compound

Procedure

The title compound was prepared from 2-hydrazinyl-5-((2-methoxyethoxy)methyl)pyridine and isothiocyanatobenzene following the procedure described in the synthesis of compound 4A.

Sources & evidence

ORD record: ord-e6dfdedf851c4d1f831bffaad4a29239
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08178534B2

Reaction notes

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