Salicylaldehyde → HCID 22495454, compound

HRID 1935362

Reaction equation

HRID 1935362 reaction equation
C1(C)C=CC(S([N:10]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14][N:13](S(C3C=CC(C)=CC=3)(=O)=O)[CH2:12][CH2:11]2)(=O)=O)=CC=1.[CH:30](=O)[C:31]1[C:32](=[CH:34][CH:35]=[CH:36][CH:37]=1)[OH:33]>[H][H].O=[Pt]=O>[OH:33][C:32]1[CH:34]=[CH:35][CH:36]=[CH:37][C:31]=1[CH2:30][N:16]1[CH2:15][CH2:14][N:13]2[CH2:12][CH2:11][N:10]([CH2:12][CH2:11][NH:10][CH2:18][CH2:17]2)[CH2:18][CH2:17]1

Participants

4

Reactant 2

HCID 6998SalicylaldehydeHCID 109062624,7-Bis(p-tolylsulphonyl)-1,4,7-triazacyclononane

Product 1

HCID 22495454HCID 22495454, compound

Reagents, catalysts & solvents 1

HCID 178506448HCID 178506448, compoundCatalyst

Procedure

From 1,4,7,10-tetrazabicyclo[5.5.2]tetradecane (1.1.20), salicylaldehyde (1.5 equivalents) and H2/PtO2.

Sources & evidence

ORD record
ord-5cc7709358d34033b20a5aab83ec0197
Source dataset
uspto-grants-2002_05
Patent number
US06387891B2

Linked notes

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