Hydrochloric Acid → 2',4',6'-Triamino-4-methylbiphenyl

HRID 1976501

Reaction equation

[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-])=O)[CH:7]=[C:6]([N+:13]([O-])=O)[C:5]=1[C:16]1[CH:21]=[CH:20][C:19]([CH3:22])=[CH:18][CH:17]=1)([O-])=O.Cl>>[NH2:1][C:4]1[CH:9]=[C:8]([NH2:10])[CH:7]=[C:6]([NH2:13])[C:5]=1[C:16]1[CH:21]=[CH:20][C:19]([CH3:22])=[CH:18][CH:17]=1

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 223420002',4',6'-Trinitro-4-methylbiphenyl

Product 1

HCID 223419982',4',6'-Triamino-4-methylbiphenyl

Procedure

2′,4′,6′-trinitro-4-methylbiphenyl (1) is reacted with stannous chloride and hydrochloric acid to yield 2′,4′,6′-triamino-4-methylbiphenyl (2).

Sources & evidence

ORD record: ord-ac9341e0ba614126adfaec061049b2da
Source dataset: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06226352B1

Linked notes

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