HCID 178469423, compound → 6-fluoro-1H-1,2,3-benzotriazole-7-carboxylic acid
Reaction equation
[F:1][C:2]1[CH:3]=[CH:4][C:5]2[N:9]=[N:8][NH:7][C:6]=2[C:10]=1[C:11]([O:13]CC)=[O:12]>Cl>[F:1][C:2]1[CH:3]=[CH:4][C:5]2[N:9]=[N:8][NH:7][C:6]=2[C:10]=1[C:11]([OH:13])=[O:12]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
ethyl 6-fluoro-1H-1,2,3-benzotriazole-7-carboxylate (920 mg) was heated in 6N HCl until all of the starting material disappeared. Evaporation of the HCl afforded 718 mg of a brownish solid.
Workup
- customEvaporation of the HCl
Sources & evidence
- ORD record
- ord-ff9efc54638b4c7f8f76bd61ed0e16db
- Source dataset
- uspto-grants-2010_01
- Patent number
- US07645771B2
Reaction notes
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