P,P-Diphenyl-N-(phenylmethylene)phosphinic amide → HCID 178527071, compound

HRID 2030522Notes

Reaction equation

HRID 2030522 reaction equation
[O:1]=[P:2]([c:17]1[cH:22][cH:21][cH:20][cH:19][cH:18]1)([c:11]2[cH:16][cH:15][cH:14][cH:13][cH:12]2)\[N:3]=[CH:4]\[c:5]3[cH:10][cH:9][cH:8][cH:7][cH:6]3.C[C:23]1(C(C)(C)OB(CB2OC(C)(C)C(C)(C)O2)[O:24]1)C>>[OH:24][CH2:23][CH:4]([c:5]1[cH:10][cH:9][cH:8][cH:7][cH:6]1)[NH:3][P:2]([c:17]2[cH:22][cH:21][cH:20][cH:19][cH:18]2)([c:11]3[cH:16][cH:15][cH:14][cH:13][cH:12]3)=[O:1]

Participants

9

Reactant 2

HCID 608413P,P-Diphenyl-N-(phenylmethylene)phosphinic amideHCID 113116854,4,5,5-Tetramethyl-2-((tetramethyl-1,3,2-dioxaborolan-2-yl)methyl)-1,3,2-dioxaborolane

Product 1

HCID 178527071HCID 178527071, compound

Reagents, catalysts & solvents 6

HCID 236647642-Propanol, 2-methyl-, lithium salt (1:1)ReagentHCID 23676751Interox A; PerasafeReagentHCID 4189906(S)-(-)-2,2'-Bis(di-p-tolylphosphino)-1, 1'-binaphthylCatalystHCID 11068737tetrakis(acetonitrile)copper(I) hexafluorophosphateCatalystHCID 1140TolueneSolventHCID 117669-PhenylanthraceneInternal standard

Conditions

Temperature
50 °C

Sources & evidence

ORD record
ord-38adaf6db3d449ada6a0d01386ff210a
Source dataset
39k HTE dataset from Pfizer
Original link
View source

Reaction notes

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