Hydrochloric Acid → Tris(aminomethyl)phosphine oxide trihydrochloride
Reaction equation
[N:1]12C[N:5]3[CH2:6][P:7](=[O:10])([CH2:9][N:3](C3)C1)[CH2:8]2.[ClH:12]>O>[ClH:12].[ClH:12].[ClH:12].[NH2:5][CH2:6][P:7](=[O:10])([CH2:9][NH2:3])[CH2:8][NH2:1]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Following the procedure outline in Example 6, the 1,3,5-triaza-7-phosphaadamantane-7-oxide (7.92 g, 0.04 mol) was hydrolyzed with a solution of 22 g (0.22 mol) of 37.7% hydrochloric acid and 80 g of water, giving, after workup, 5.9 g (60% yield) of tris(aminomethyl)phosphine oxide trihydrochloride, dec. 239° C. without melting.
Workup
- customgiving
Sources & evidence
- ORD record
- ord-7f7687a32ad243e485ef272f106fa321
- Source dataset
- uspto-grants-1980_04
- Patent number
- US04196149
Reaction notes
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