HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → Piperidinium 2,4-Dioxo-5-(2-tritylaminothiazol-4-ylmethylene)thiazolidine-3-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | (2,4-Dioxo-1,3-thiazolidin-3-yl)acetic acid | HCID 2770836 | — |
| Reactant | 2-(Tritylamino)thiazole-4-carbaldehyde | HCID 15053569 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Piperidinium 2,4-Dioxo-5-(2-tritylaminothiazol-4-ylmethylene)thiazolidine-3-acetate | HCID 73454615 | — |
Reaction Steps
Following a procedure similar to that described in Example 17, the desired compound was prepared from 2.3 g of 2-tritylaminothiazole-4-carbaldehyde, 0.9 g of 2,4-dioxothiazolidine-3-acetic acid, 0.9 g of piperidine and 20 ml of ethanol. The resulting product was a pale yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-721fbfc7608c4142b3334da359872d35 |
| Source note | uspto-grants-1990_06 |