Glyceryl 1-phosphate → Pipes

HRID 2201170

Reaction equation

HRID 2201170 reaction equation
[CH2:1]1[N:6]([CH2:7][CH2:8][S:9]([OH:12])(=[O:11])=[O:10])[CH2:5][CH2:4]O[CH2:2]1.[CH3:13][C:14]1[N:19](C)N(C2C=CC=CC=2)C(=O)C=1N.P(OCC(O)CO)(O)(O)=O.[N-]=[N+]=[N-].[Na+].C[C@@H]([C@@H]1[C@@]2(C)[C@@H](O)C[C@@H]3[C@@]4(C)CC[C@@H](O)C[C@H]4C[C@@H](O)[C@@]3(C)[C@@H]2CC1)CCC([O-])=O.[Na+].C(OC1C=CC=CC=1)CCCCCCCC.C(OCCCCCCCCCCCC)CCCCCCCCCCC>OCC(CO)O>[CH2:2]1[N:19]([CH2:14][CH2:13][S:9]([OH:12])(=[O:11])=[O:10])[CH2:4][CH2:5][N:6]([CH2:7][CH2:8][S:9]([OH:12])(=[O:11])=[O:10])[CH2:1]1

Participants

9

Reactant 7

HCID 754Glyceryl 1-phosphateHCID 21514-AminoantipyrineHCID 20667Dilauryl EtherHCID 33557Sodium AzideHCID 781654-Morpholineethanesulfonic acidHCID 9859302Benzene, (nonyloxy)-HCID 44582063sodium (4R)-4-[(3R,5S,7R,8R,9R,10S,12S,13R,14R,17R)-3,7,12-trihydroxy-8,10,13-trimethyl-1,2,3,4,5,6,7,9,11,12,14,15,16,17-tetradecahydrocyclopenta[a]phenanthren-17-yl]pentanoate

Product 1

HCID 79723Pipes

Reagents, catalysts & solvents 1

HCID 753GlycerolSolvent

Procedure

MES (Dojindo Laboratories); EMSE (Daito Chemix Corporation); 4-aminoantipyrine (Saikyo Kasei), CEBP-M (enzyme having an activity of lipoprotein lipase; Asahi Kasei Corporation); GYK-301 (glycerol kinase; Toyobo Co., Ltd.); GPOM (glycerol 3-phosphate oxidase; Asahi Kasei Corporation), catalase (Sigma), peroxidase (Toyobo Co., Ltd.), sodium azide (Kanto Chemicals Co., Inc.), Emulgen B66 (Kao Corporation), Newcol 610 (Nippon Nyukazai Co., Ltd.), Newcol 2608F (Nippon Nyukazai Co., Ltd.), New Calgen GP120 (Takemoto Oil & Fat, Co. Ltd.), NIKKOL R1020 (Nikko Chemicals Co., Ltd.), Emulgen A60 (Kao Corporation), BLAUNON DSP12.5 (Aoki Oil Industrial Co., Ltd.), HI-TENOL N08 (Daichi Kogyo Co., Ltd.), Emulgen L40 (Kao Corporation), Newcol 707SF (Nippon Nyukazai Co., Ltd.), Wondersurf S1400 (Aoki Oil Industrial Co., Ltd.), New Calgen E150 (Takemoto Oil & Fat, Co. Ltd.), Sodium cholate (Acros), Emulgen 909 (POE nonylphenyl ether HLB 12.4; Kao Corporation), Emulmin NL70 (POE lauryl ether HLB 12.4; Sanyo Chemicals Industries, Ltd.).

Sources & evidence

ORD record
ord-cf4a34f5e52845f1b0a21fe822979c93
Source dataset
uspto-grants-2016_06
Patent number
US09360432B2

Linked notes

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