Methane → HCID 178419113, compound

HRID 2220036

Reaction equation

HRID 2220036 reaction equation
[B:1]12[B:4]3[B:5]4[B:2]1[C:3]234.[O-2:6].[O-2].[Ti+4:8].[CH4:9].[C-]#[Si+]>CO>[B:1]12[B:4]3[B:5]4[B:2]1[C:3]234.[O-2:6].[O-2:6].[Ti+4:8].[C:9]

Participants

6

Reactant 4

HCID 297MethaneHCID 9863Silicon carbideHCID 123279Boron carbideHCID 162651Titanium oxide (Ti3O)

Product 1

HCID 178419113HCID 178419113, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To the boron carbide powder, 14.5 mol % of the submicron-size or nano-size titanium dioxide powder and 21.5 mol % of carbon black were incorporated, and using a methanol solvent, mixing was carried out by a planetary ball mill made of silicon carbide (SiC) at a rotational speed of 270 rpm for 1 hour, followed by drying by a evaporator and further by drying at 150° C. for 24 hours. Then, the mixture was sieved through a sieve with an opening of 250 μm to obtain a boron carbide-titanium dioxide-carbon mixed powder.

Workup

  1. additionmixing
  2. customby drying by a evaporator
  3. customfurther by drying at 150° C. for 24 hours
  4. filtrationThen, the mixture was sieved through a sieve with an opening of 250 μm

Sources & evidence

ORD record
ord-527f550cf19a465ea96d73a4b1382069
Source dataset
uspto-grants-2008_08
Patent number
US07417002B2

Linked notes

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