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Hydrochloric Acid → HCID 23330494, compound

HRID 224827
Notes
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Reaction equation

HRID 224827 reaction equation
C([N:4]1[CH2:8][CH2:7][N:6]=[C:5]1[NH:9][C:10]1[N:14]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[N:13]=[C:12]([CH3:21])[CH:11]=1)(=O)C.[ClH:22]>CO>[ClH:22].[CH3:21][C:12]1[CH:11]=[C:10]([NH:9][C:5]2[NH:6][CH2:7][CH2:8][N:4]=2)[N:14]([C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)[N:13]=1
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

4

Reactant 2

HCID 313Hydrochloric Acid2×HCID 12763795HCID 12763795, compound

Product 1

HCID 23330494HCID 23330494, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1-Acetyl-2-(3-methyl-1-phenyl-5-pyrazolyl) amino-2-imidazoline (35.0 g.) was treated with HCl in methanol as described in Example II to give 28.7 g. product as the hydrochloride. mp 182°-184°

Workup

  1. customto give 28.7 g

Sources & evidence

ORD record
ord-a791e2aa46f94f3fa9afc23b6d50b91e
Source dataset
uspto-grants-1980_11
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04234594

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes