Hydrazine hydrate (1:1) → 7-Phenylheptan-1-amine
Reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N:14]2C(=O)C3C(=CC=CC=3)C2=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NN.O>C(O)C>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Batch size: 11.0 g (34.2 mmol) 2-(7-phenyl-heptyl)-isoindol-1,3-dione and 3.4 g (68.4 mmol) hydrazine.hydrate in 100 ml ethanol.
Sources & evidence
- ORD record
- ord-b605a74308d947568078c36829d66805
- Source dataset
- uspto-grants-2008_01
- Patent number
- US07320993B1
Reaction notes
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