Chloroacetyl chloride → 3-(1-Ethyl-1-cyclohexyloxycarbonyl)propyl methacrylate

HRID 225397

Reaction equation

C([C:3]1([OH:13])[CH:10]2[CH2:11]C3CC(CC1C3)[CH2:9]2)C.ClCC(Cl)=[O:17].[CH2:19]([C:21]1([OH:27])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1)[CH3:20].Cl[CH2:29][CH2:30][CH2:31][C:32](Cl)=[O:33]>>[C:3]([O:13][CH2:29][CH2:30][CH2:31][C:32]([O:27][C:21]1([CH2:19][CH3:20])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1)=[O:33])(=[O:17])[C:10]([CH3:11])=[CH2:9]

Participants

Reactant 4

HCID 6577Chloroacetyl chloride

HCID 160211-Ethylcyclohexanol

HCID 783704-Chlorobutyryl chloride

HCID 44019512-Ethyl-2-adamantanol

Product 1

HCID 689528853-(1-Ethyl-1-cyclohexyloxycarbonyl)propyl methacrylate

Procedure

Synthetic experiment was conducted in the same manner as in Monomer Synthesis Example 1 except that 2-ethyl-2-adamantanol and chloroacetyl chloride were changed to 1-ethyl-1-cyclohexanol and 4-chlorobutyryl chloride respectively, and the above described methacrylic derivative was obtained.

Workup

customwas obtained

Sources & evidence

ORD record: ord-93c258ea3b8e46caab312e8f5ccd8886
Source dataset: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07556908B2

Linked notes

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