O-Xylene → HCID 18788042, compound

HRID 2258381

Reaction equation

HRID 2258381 reaction equation
[CH2:1]([N:5](CC(C)=C)[C:6]1[CH:11]=CC=C[CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:16]1([CH3:23])[C:17](C)=[CH:18][CH:19]=[CH:20][CH:21]=1>[Cl-].[Zn+2].[Cl-]>[CH2:1]([N:5]1[C:17]2[C:16](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:23][C:6]1([CH3:11])[CH3:7])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 7237O-XyleneHCID 54010992N-butyl-N-(2-methylprop-2-eneyl)aniline

Product 1

HCID 18788042HCID 18788042, compound

Reagents, catalysts & solvents 1

HCID 3007855ZincchlorideCatalyst

Procedure

A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).

Workup

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationThe cooled mixture was filtered
  4. customthe organic phase evaporated

Sources & evidence

ORD record
ord-7f603290ea884b37aa05920e12f26970
Source dataset
uspto-grants-1997_08
Patent number
US05660598

Linked notes

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