Methacryloyl chloride → 4-Benzoylphenyl methacrylate

HRID 2292201

Reaction equation

HRID 2292201 reaction equation
[OH:1][C:2]1[CH:15]=[CH:14][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[C:16](Cl)(=[O:20])[C:17]([CH3:19])=[CH2:18]>N1C=CC=CC=1>[C:16]([O:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:14][CH:15]=1)(=[O:20])[C:17]([CH3:19])=[CH2:18]

Participants

4

Reactant 2

HCID 13528Methacryloyl chlorideHCID 143474-Hydroxybenzophenone

Product 1

HCID 112308954-Benzoylphenyl methacrylate

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Prepared from 6.0 g of 4-hydroxybenzophenone and 4.4 ml of methacryloyl chloride in 70 ml of pyridine. Recrystallized from ethyl acetate-ethanol-water; M.P.~69.5°-70.5° C.

Workup

  1. customRecrystallized from ethyl acetate-ethanol-water

Sources & evidence

ORD record
ord-1acdee1fb46248e9a9aa8eaed28885da
Source dataset
uspto-grants-1989_01
Patent number
US04801610

Linked notes

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