Potassium Carbonate → HCID 21477968, compound
Reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].C(=O)([O-])[O-].[K+].[K+].[F:15][C:16]1[C:21]([F:22])=[C:20]([CH:23]2[O:28][CH2:27][CH:26]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])[CH2:25][O:24]2)[CH:19]=[CH:18][C:17]=1[OH:38]>>[F:22][C:21]1[C:16]([F:15])=[C:17]([O:38][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH:18]=[CH:19][C:20]=1[CH:23]1[O:24][CH2:25][CH:26]([CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])[CH2:27][O:28]1Participants
4
Procedure
Quantities: 1-bromoheptane (0.31 g, 1.46 mmol), potassium carbonate (0.4 g, 3 mmol) and compound from Example 126 (0.Sg, 1.46 mmol). The experimental procedure was as described in Example 38.
Sources & evidence
- ORD record
- ord-6d295522e5124ca58bdf5f3c0b0e52db
- Source dataset
- uspto-grants-1997_11