HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4,5,6-Pentafluorobenzyl Alcohol → 2,3,4,5,6-Pentafluorobenzyl 5-amino-4-oxopentanoate Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4,5,6-Pentafluorobenzyl Alcohol | HCID 9923 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | 2,3,4,5,6-Pentafluorobenzyl 5-amino-4-oxopentanoate Hydrochloride | HCID 17989822 | — |
Reaction Steps
From 2,3,4,5,6-pentafluorobenzyl alcohol (5.1 g; 26 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol). The reaction was complete after 6 days at 100° C. The yield was 0.25 g (13%). Mp 146-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563819B1 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a5df7938c9714110acc503e506bc4e72 |
| Source note | uspto-grants-2009_07 |