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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 234071Generated: October 27, 2026

1,3-Bis(4-methylphenyl)prop-2-en-1-one → 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene

https://huagongshe.com/reaction/234071

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Bis(4-methylphenyl)prop-2-en-1-oneHCID 256552—
CatalystPalladiumHCID 23938—
SolventAcetic AcidHCID 176—
Product1-Methyl-4-[3-(4-methylphenyl)propyl]benzeneHCID 57172699.4%

Reaction Steps

To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05594081
Source datasetuspto-grants-1997_01
ORD IDord-9c59153766d74092b67b123096222700
Source noteuspto-grants-1997_01