Acetic Acid → 4-(Dimethylamino)Benzaldehyde

HRID 234865

Reaction equation

[CH3:1][N:2]([C:4]1[CH:9]=[CH:8][C:7](N=NC2C=CC=CC=2)=[CH:6][CH:5]=1)[CH3:3].Cl(O)(=O)(=O)=O.[C:23](O)(=[O:25])C>>[CH3:3][N:2]([C:4]1[CH:5]=[CH:6][C:7]([CH:23]=[O:25])=[CH:8][CH:9]=1)[CH3:1]

Participants

Reactant 3

HCID 176Acetic Acid

HCID 6053C.I. Solvent Yellow 2

HCID 24247Perchloric Acid

Product 1

HCID 74794-(Dimethylamino)Benzaldehyde

Procedure

Ehrlichs Reagent is prepared by mixing 10 g DMAB with 420 ml glacial acetic acid, and 80 ml perchloric acid.

Sources & evidence

ORD record: ord-05a03bdb336147d5be9d763e86734481
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05597702

Linked notes

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