Methanol → HCID 54335577, compound
Reaction equation
[CH2:1]([S:7][CH:8]=[CH:9][CH2:10]Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].C(N(C(C)C)CC)(C)C.[CH3:21][OH:22]>CCCCCC>[CH3:21][O:22][CH2:10][CH:9]=[CH:8][S:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
3-Hexylthio-2-propenyl chloride is added to a solution of diisopropyl ethyl amine (3.68 g, 28.5 mmol) in 20 ml of methanol. The mixture is stirred overnight at RT. It is then diluted with hexane, washed with water and with brine and is stripped. The crude product is purified by prep. TLC to give 3-methoxy-1-hexylthio-1-propene.
Workup
- washwashed with water and with brine
- customThe crude product is purified by prep
Sources & evidence
- ORD record
- ord-3f5b6b6e640848808e565dc80061b09b
- Source dataset
- uspto-grants-1989_10
- Patent number
- US04877899
Reaction notes
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