Reaction equation
[Li:1][CH2:2][CH2:3][CH2:4][CH3:5].Br[C:7]1[CH:14]=CC=C[C:8]=1[CH:9]=C.C1COCC1>C(OCC)C>[Li:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:14][C:3]=1[CH:4]=[CH2:5]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A 0.35M solution of 2-lithiostyrene was prepared dropwise addition of nBuLi to a -78° C. solution of 2-bromostyrene in 5:1 THF:diethyl ether.
Sources & evidence
- ORD record
- ord-bf6097d0b83a440d8d2344038fdda671
- Source dataset
- uspto-grants-1997_01
- Patent number
- US05597931
Linked notes
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