HCID 86664895, compound → HCID 86664894, compound
Reaction equation
[NH2:1][C:2]1[C:11]([N+:12]([O-])=O)=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[C:4]([O:15][CH2:16][CH:17]([F:19])[F:18])[N:3]=1>[Ni].C1COCC1.CO>[NH2:12][C:11]1[C:2]([NH2:1])=[N:3][C:4]([O:15][CH2:16][CH:17]([F:19])[F:18])=[C:5]([CH:10]=1)[C:6]([O:8][CH3:9])=[O:7]Participants
5
Reactant 1
Product 1
Reagents, catalysts & solvents 3
Procedure
Prepared analogously to example 154d by hydrogenation of the product obtained in (803a) using Raney nickel in THF and methanol.
Workup
- customPrepared analogously to example 154d by hydrogenation of the product
Sources & evidence
- ORD record
- ord-76c832c10d45413d85790f1a60ca1110
- Source dataset
- uspto-grants-2014_04
- Patent number
- US08703796B2
Reaction notes
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