Water → N-heptyl galactosylamine

HRID 2379382

Reaction equation

HRID 2379382 reaction equation
O[C@@H:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4].[CH2:13]([NH2:20])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].O>>[CH2:13]([NH:20][CH:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

4

Reactant 3

HCID 962WaterHCID 81271-HeptanamineHCID 439353beta-D-Galactopyranose

Product 1

HCID 18656114N-heptyl galactosylamineYield 87%

Procedure

β-D-galactose (10 g, 1 eq), heptylamine (7.7 g, 1 eq) and water (2 g, 3 eq) were heated in a reaction flask at 80° C. for about 15 minutes. The sample was filtered and washed as described for the decyl derivative to give an 87% yield.

Workup

  1. filtrationThe sample was filtered
  2. washwashed
  3. customto give an 87% yield

Sources & evidence

ORD record
ord-c02daafaceb7448fa865308ce59b8af7
Source dataset
uspto-grants-1994_11
Patent number
US05362480

Linked notes

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