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3,5-Dichloroaniline → 3,5-dibromo-N-(3,5-dichlorophenyl)-2-hydroxybenzamide

HRID 2384438
Notes
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Reaction equation

HRID 2384438 reaction equation
[Br:1][C:2]1[CH:10]=[C:9]([Br:11])[CH:8]=[C:4]([C:5]([OH:7])=O)[C:3]=1[OH:12].[Cl:13][C:14]1[CH:15]=[C:16]([CH:18]=[C:19]([Cl:21])[CH:20]=1)[NH2:17]>>[Br:1][C:2]1[C:3]([OH:12])=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([NH:17][C:16]1[CH:15]=[C:14]([Cl:13])[CH:20]=[C:19]([Cl:21])[CH:18]=1)=[O:7]
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 122813,5-DichloroanilineHCID 184643,5-Dibromosalicylic acid

Product 1

HCID 178602243,5-dibromo-N-(3,5-dichlorophenyl)-2-hydroxybenzamideYield 44.2%

Procedure

Using 3,5-dibromosalicylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.

Sources & evidence

ORD record
ord-b21ee62f62774df8b60274c41eb38a2b
Source dataset
uspto-grants-2012_09
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US08263657B2

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes