Ethanol → Ethyl sulfoacetate

HRID 2396092

Reaction equation

HRID 2396092 reaction equation
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Participants

3

Reactant 2

HCID 702EthanolHCID 31257Sulfoacetic acid

Product 1

HCID 12216623Ethyl sulfoacetate

Procedure

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

Workup

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

Sources & evidence

ORD record
ord-292b72945d0e454c82fdb19175274c63
Source dataset
uspto-grants-1996_02
Patent number
US05491170

Linked notes

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