Beta-Alanine → Magnesium beta-alaninate

HRID 2397425Notes

Reaction equation

HRID 2397425 reaction equation
[NH2:1][CH2:2][CH2:3][C:4]([OH:6])=[O:5].C(=O)([O-])[O-].[Mg+2:11].C(C(C(C([O-])=O)O)O)([O-])=O.[Na+].[Na+].OCl>O>[NH2:1][CH2:2][CH2:3][C:4]([O-:6])=[O:5].[Mg+2:11].[NH2:1][CH2:2][CH2:3][C:4]([O-:6])=[O:5]

Participants

6

Reactant 4

HCID 239Beta-AlanineHCID 11029Magnesium CarbonateHCID 13355Disodium 2,3-dihydroxybutanedioateHCID 24341Hypochlorous Acid

Product 1

HCID 86734646Magnesium beta-alaninate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Magnesium β-alaninate was prepared by reacting 3.6 g. of β-alanine with 1.8 g. of basic magnesium carbonate in 40 g. of water, while agitating at 75° C. for one half hour. To the cooled slurry was added 2.5 g. of sodium tartrate. After five minutes of stirring, 80 g. of zirconyl hydroxychloride solution (14.4% Zr) was added to the above slurry with agitation. The solution cleared on stirring and had a final pH of 3.3. The product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg and found to contain 33.1% Zr, 1.3% Mg, 1.4% Na, and 10.3% β-alanine.

Workup

  1. additionTo the cooled slurry was added 2.5 g
  2. stirringon stirring
  3. customThe product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg

Sources & evidence

ORD record
ord-b3bf4ff98d5d423ca9f2dfaaecf2f5b2
Source dataset
uspto-grants-1977_05
Patent number
US04021536

Reaction notes

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