Benzoic Acid → HCID 178443205, compound

HRID 2403125Notes

Reaction equation

HRID 2403125 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([OH:32])(=[O:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1.[OH2:33]>CC(C)=O>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([O-:32])(=[O:31])[C:25]1[C:30](=[CH:29][CH:28]=[CH:27][CH:26]=1)[OH:33]

Participants

5

Reactant 3

HCID 243Benzoic AcidHCID 962WaterHCID 2330Benzalkonium

Product 1

HCID 178443205HCID 178443205, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Benzalkonium saccharinate (0.01 mol) and benzoic acid (0.01 mol) were dissolved in 25 mL of hot acetone. The mixture was stirred at room temperature for 5 h. Distilled water was added. The organic phase was separated and washed with distilled water. Organic phase was evaporated and the product, benzalkonium salicylate, was dried under vacuum. 1H and 13C NMR (DMSO) were obtained.

Workup

  1. customThe organic phase was separated
  2. washwashed with distilled water
  3. customOrganic phase was evaporated
  4. dry with materialthe product, benzalkonium salicylate, was dried under vacuum
  5. custom1H and 13C NMR (DMSO) were obtained

Sources & evidence

ORD record
ord-3323f506f78c4f2ca2530abb2a35cff9
Source dataset
uspto-grants-2014_08
Patent number
US08802596B2

Reaction notes

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