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Potassium Iodide → HCID 19838229, compound

HRID 2414027
Notes
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Reaction equation

HRID 2414027 reaction equation
[C:1]1([CH2:7][O:8][C:9]2[CH:10]=[C:11]([CH2:23][CH2:24][NH:25][CH2:26][C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=3)[CH:12]=[CH:13][C:14]=2[O:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Br[CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][C:39]([O:41][CH2:42][CH3:43])=[O:40].C(=O)([O-])[O-].[K+].[K+].[I-].[K+]>C(#N)C>[CH2:42]([O:41][C:39](=[O:40])[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][N:25]([CH2:24][CH2:23][C:11]1[CH:12]=[CH:13][C:14]([O:15][CH2:16][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)=[C:9]([O:8][CH2:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:10]=1)[CH2:26][C:27]1[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1)[CH3:43]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

6

Reactant 4

HCID 4875Potassium IodideHCID 11430Potassium CarbonateHCID 117544Ethyl 6-bromohexanoateHCID 19838166HCID 19838166, compound

Product 1

HCID 19838229HCID 19838229, compound

Reagents, catalysts & solvents 1

HCID 6342
Acetonitrile
Solvent

Procedure

A suspension of 3,4-bis(phenylmethoxy)-N-phenylmethyl benzeneethanamine (10 g), ethyl 6-bromohexanoate (10.5 g), potassium carbonate (6.34 g) and potassium iodide (1 g) in acetonitrile (250 ml) was heated under reflux for 24 hours.

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for 24 hours

Sources & evidence

ORD record
ord-35a258355d264c36a9c3834cbb16c3a7
Source dataset
uspto-grants-1988_01
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04720586

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes