Hydrochloric Acid → 3,7-Diazabicyclo(3.3.1)nonane

HRID 2414719

Reaction equation

HRID 2414719 reaction equation
C([N:8]1[CH2:15][CH:14]2[CH2:16][CH:10]([CH2:11][N:12](CC3C=CC=CC=3)[CH2:13]2)[CH2:9]1)C1C=CC=CC=1.Cl>C(O)C.[Pd]>[CH:10]12[CH2:16][CH:14]([CH2:13][NH:12][CH2:11]1)[CH2:15][NH:8][CH2:9]2

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 473413,7-Dibenzyl-3,7-diazabicyclo[3.3.1]nonane2×

Product 1

HCID 1927203,7-Diazabicyclo(3.3.1)nonane

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

Obtainable by catalytic hydrogenation of 3,7-dibenzyl-3.7-diazabicyclo[3.3.1]nonane. Hydrogenation is performed by stirring 3,7-dibenzyl-3.7-diazabicyclo[3.3.1]nonane in a mixture of ethanol, concentrated hydrochloric acid and palladium on carbon under an atmosphere of hydrogen.

Sources & evidence

ORD record
ord-086638eac38148288e311dcd759159cf
Source dataset
uspto-grants-2004_11
Patent number
US06815438B2

Linked notes

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