Sodium Iodide → HCID 178502576, compound

HRID 2419955

Reaction equation

HRID 2419955 reaction equation
[CH3:1][O:2][C:3]([P:5](=[O:12])([O:9][CH2:10][CH3:11])[O:6]CC)=[O:4].[I-].[Na+:14]>O1CCCC1>[CH3:1][O:2][C:3]([P:5](=[O:6])([OH:12])[OH:9])=[O:4].[CH2:10]([Na:14])[CH3:11]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 170573Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide

Product 1

HCID 178502576HCID 178502576, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123° d.

Workup

  1. filtrationThe resulting mixture was filtered

Sources & evidence

ORD record
ord-04a7421230c04887bbc12f7c2e1c8d77
Source dataset
uspto-grants-1978_08
Patent number
US04108626

Linked notes

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