Methyl Anthranilate → HCID 178497641, compound

HRID 24734

Reaction equation

HRID 24734 reaction equation
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6](=[C:13](OCC)[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:5]1=[O:23])(=O)C.[C:24]([O:33][CH3:34])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[NH2:27].[OH-].[Na+]>CN(C=O)C.CO>[CH3:34][O:33][C:24]([C:25]1[CH:31]=[CH:30][CH:29]=[CH:28][C:26]=1[NH:27]/[C:13](=[C:6]1\[C:5](=[O:23])[NH:4][C:12]2[C:7]\1=[CH:8][CH:9]=[CH:10][CH:11]=2)/[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)=[O:32]

Participants

6

Reactant 3

HCID 8635Methyl AnthranilateHCID 14798Sodium HydroxideHCID 542378881-Acetyl-3-(1-ethoxy-1-phenylmethylidene}-2-indolinone

Product 1

HCID 178497641HCID 178497641, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to Example 1 from 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone and methyl anthranilate in DMF and subsequent brief treatment with sodium hydroxide solution in methanol.

Sources & evidence

ORD record
ord-a680a449b4dd4baa87869b79b033a3b1
Source dataset
uspto-grants-2005_02
Patent number
US06855710B2

Linked notes

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