p-Toluenesulfonic acid → Benzyl 2-mercaptopropanoate

HRID 256235

Reaction equation

HRID 256235 reaction equation
[SH:1][CH:2]([CH3:6])[C:3]([OH:5])=[O:4].[C:7]1([CH3:17])[CH:12]=[CH:11][C:10](S(O)(=O)=O)=[CH:9][CH:8]=1>>[CH2:17]([O:4][C:3](=[O:5])[CH:2]([SH:1])[CH3:6])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1

Participants

3

Reactant 2

HCID 6101p-Toluenesulfonic acidHCID 62326(+-)-2-Mercaptopropionic acid

Product 1

HCID 10442670Benzyl 2-mercaptopropanoate

Procedure

Into a 100 ml reaction flask equipped with thermometer, reflux condenser, hot plate (equipped with magnetic stirring apparatus) and spin bar are placed 21.6 grams benzyl alchol; 29.6 grams of 2-mercaptopropionic acid; and 0.5 grams of para-toluene sulphonic acid.

Workup

  1. customInto a 100 ml reaction flask
  2. customequipped with thermometer
  3. temperaturereflux condenser
  4. customhot plate (equipped with magnetic stirring apparatus)

Sources & evidence

ORD record
ord-55d04f41ef3d4183981caab8ce50a34e
Source dataset
uspto-grants-1987_10
Patent number
US04701548

Linked notes

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