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Putrescine → HCID 178511050, compound

HRID 262699
Notes
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Reaction equation

HRID 262699 reaction equation
[C:1](=[S:3])=[O:2].[NH2:4][CH2:5][CH2:6][CH2:7][CH2:8][NH2:9]>O.C(O)C>[NH2:4][CH2:5][CH2:6][CH2:7][CH2:8][NH:9][C:1](=[S:3])[OH:2]
ParticipantsProcedureSources & evidenceReaction notes

Participants

5

Reactant 2

HCID 1045PutrescineHCID 10039Carbonyl Sulfide

Product 1

HCID 178511050HCID 178511050, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

passing carbonyl sulfide gas into a solution of tetramethylene diamine dissolved in a mixture of water and ethanol in equal proportions by weight at a temperature of from about 30° C. to about 45° C. to form N-(4-aminobutyl)thiocarbamic acid or zwitterion thereof; and

Sources & evidence

ORD record
ord-504a7a055f8e4316914c9a3558fd99b6
Source dataset
uspto-grants-1979_05
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04154931

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes