Hydrochloric Acid → 2-[Butyl(methyl)amino]ethan-1-ol--hydrogen chloride (1/1)
Reaction equation
[ClH:1].[CH3:2][N:3]([CH2:8][CH2:9][OH:10])[CH2:4][CH2:5][CH2:6][CH3:7]>C(OCC)C>[ClH:1].[CH3:2][N:3]([CH2:8][CH2:9][OH:10])[CH2:4][CH2:5][CH2:6][CH3:7]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Hydrochloric acid (gas) was bubbled through a solution of 10.0 g (0.0762 mmol) of 2-(N-methyl-N-butylamino)ethanol in diethyl ether. The resultant solution was concentrated in vacuo to provide a gold oil.
Workup
- concentrationThe resultant solution was concentrated in vacuo
- customto provide a gold oil
Sources & evidence
- ORD record
- ord-e81260f2187b416f97980818ba9de356
- Source dataset
- uspto-grants-1997_07
- Patent number
- US05652213
Reaction notes
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