Hydroxylamine → p-Chlorobenzylmercaptoacetohydroxamic acid
Reaction equation
[Cl:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][S:7][CH2:8][C:9](OC)=[O:10])=[CH:4][CH:3]=1.[NH2:15][OH:16].CO[Na]>CO>[Cl:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][S:7][CH2:8][C:9]([NH:15][OH:16])=[O:10])=[CH:4][CH:3]=1Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 0.15 mol of methyl p-chlorobenzylmercapto-acetate in 50 ml of methanol is mixed with a solution of 0.225 mol of hydroxylamine (base) and 0.15 mol of CH3ONa in 150 ml of methanol.
Sources & evidence
- ORD record
- ord-efaa9b4c7b1c4dcb9527ca58e78e2040
- Source dataset
- uspto-grants-1979_04
- Patent number
- US04151300
Reaction notes
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